Section 100 in The Rajasthan Distilleries Rules, 1977
100. c.c. of the sample are to be slowly heated in a small copper flask fitted with a glass fractionating column 7 inches high and 3½ inches in diameter, filled to the extent of 4 inches of its height with small glass beads provided with a thermometer placed opposite the exit tube about an inch above the beads, and connected with a spiral condenser. Not more than 10 c.c. of distillate should be collected in the receiver when the thermometer in the fractionating column marks a temperature of just under 149 degree F (65 degree C) from 80 c.c. to 85 c.c. should pass over between 149 degree F (65 degree C) and 162 degree F (72.2 degree C) and a total quantity of 97 degree c.c. to 98 degree c.c. should have been passed over before the thermometer marks 212 degree F (100 degree C).
