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The process consists of two steps: first chlorination followed by sublimation.
One production batch requires about 12 hrs and produces 100-110 Kg product.
The reactor used by M/s Lucky Chemicals can be converted easily to continuous reactor.
The same reactor jacket used for chilled water and high temperature is dangerous as water contamination in oil at high temperature can lead to accidents.
Present reactor temperature indicator used by Lucky Chemicals is not proper and this fact was confirmed by surface IR temperature sensor.